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The stereochemistry of transmetallation between allylstannanes and CH3SnCl3
Journal article   Peer reviewed

The stereochemistry of transmetallation between allylstannanes and CH3SnCl3

R L Marshall and David James Young
Tetrahedron Letters, Vol.33(17), pp.2369-2370
1992
url
https://doi.org/10.1016/S0040-4039(00)74214-6View
Published Version

Abstract

organotin compound
The addition of CH3SnCl3 to isomeric mixtures of allylstannane (1) proceeds stereospecifically with anti approach of the electrophile in CD2Cl2 at -78°C but is less selective in CDCl3 at room temperature. The corresponding reaction of crotyltrimethylstannane (CD2Cl2, -78°C) indicates initial γ attack. Addition of CH3SnCl3 to allyltributylstannane (CDCl3,r.t.) followed by benzaldehyde and water hydrolysis yields the expected honoallyl alcohol quantitatively. © 1992.

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