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Raman spectra of occluded cations in ZSM-5
Journal article   Peer reviewed

Raman spectra of occluded cations in ZSM-5

John R Bartlett, R P Cooney and D M Bibby
Studies in Surface Science and Catalysis, Vol.36, pp.609-614
1988
url
https://doi.org/10.1016/S0167-2991(09)60557-7View
Published Version

Abstract

Physical Chemistry (incl. Structural)
A series of ZSM-5 samples with differing framework aluminium contents (containing tetrapropylammonium cations, [TPA] +) have been characterised by Raman spectroscopy. Difference Raman spectra reveal evidence for two distinct occluded species in samples with non-zero framework aluminium content. These species have been identified as [TPA] + cations associated with framework anionic sites and non-framework anions such as Br - or OH -, on the basis of correlations between the integrated intensities of difference spectra and zeolite aluminium content. The relative abundance of the two forms have been determined semi-quantitatively and empirical evidence for [TPA] + disordering is reported.

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